tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

Base Information

Chemical Name:tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate
CAS No.:1067199-20-5
Molecular Formula:C₂₁H₂₆BrN₃O₃
Molecular Weight:448.36
Hs Code.:

Synonyms:tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

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Chemical Property of tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

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Technology Process of tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

There total 1 articles about tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1067199-19-2
tert-butyl 3-(3-(2-bromophenyl)ureido)phenylcarbamate

: 74-88-4
methyl iodide

: 1067199-20-5
tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

Guidance literature:: tert-butyl 3-(3-(2-bromophenyl)ureido)phenylcarbamate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 60h; Inert atmosphere;
DOI:10.1021/ja805758v

Reference yield: 75.0%

: 1067199-20-5
tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate

: 60011-16-7
(_S_S)-(+)-tert-butyl tert-butanethiosulfinate

: 1067199-21-6
tert-butyl 3-(3-(2-(tertbutylsulfinyl)phenyl)-1,3-dimethylureido)phenylmethylcarbamate

Guidance literature:: tert-butyl 3-(3-(2-bromophenyl)-1,3-dimethylureido)phenylmethylcarbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -90 - 20 ℃; for 0.0166667h; Inert atmosphere;

(_S_S)-(+)-tert-butyl tert-butanethiosulfinate; In tetrahydrofuran; hexane; at -90 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/ja805758v