benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

Base Information

Chemical Name:benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine
CAS No.:102998-58-3
Molecular Formula:C₂₄H₂₁ClN₂O₂
Molecular Weight:404.896
Hs Code.:

Synonyms:benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

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Chemical Property of benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

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Technology Process of benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

There total 7 articles about benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.6%

: 102998-55-0
benzyl-1 (α-methoxy-4' phenyl)ethyl-2 chloro-4 pyrrolo<3,2-c>pyridine

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 102998-58-3
benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

Guidance literature:: With trichlorophosphate; In 1,2-dichloro-ethane; at 110 ℃; for 24h;
DOI:10.1139/v86-087

Reference yield:

: 102998-41-4
benzyl-1 (α-methoxy-4' phenyl α-hydroxy)ethyl-2 chloro-4 pyrrolo<3,2-c>pyridine

: 102998-58-3
benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 68.2 percent / acetic anhydride / 20 h / Heating

2: 69 percent / H₂ / Rh on aluminum / ethanol / 48 h / Ambient temperature; at normal pressure

3: 31.6 percent / POCl₃ / 1,2-dichloro-ethane / 24 h / 110 °C

With hydrogen; trichlorophosphate; rhodium; aluminium; In ethanol; acetic anhydride; 1,2-dichloro-ethane;
DOI:10.1139/v86-087

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 102998-58-3
benzyl-1 (α-p-methoxyphenyl)ethyl-2 formyl-3 chloro-4 pyrrolo<3,2-c>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 29 percent / tert-butyllithium / diethyl ether / 1.) -65 deg C, 45 min, 2.) room temp., 1 h

2: 68.2 percent / acetic anhydride / 20 h / Heating

3: 69 percent / H₂ / Rh on aluminum / ethanol / 48 h / Ambient temperature; at normal pressure

4: 31.6 percent / POCl₃ / 1,2-dichloro-ethane / 24 h / 110 °C

With hydrogen; tert.-butyl lithium; trichlorophosphate; rhodium; aluminium; In diethyl ether; ethanol; acetic anhydride; 1,2-dichloro-ethane;
DOI:10.1139/v86-087