5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

Base Information

Chemical Name:5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid
CAS No.:31914-88-2
Molecular Formula:C₁₉H₁₇ClN₂O₅S
Molecular Weight:420.873
Hs Code.:

Synonyms:5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

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Chemical Property of 5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

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Technology Process of 5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

There total 5 articles about 5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1021869-59-9
4-chloro-2-[(2-furanylmethyl)amino]-5-[[(phenylmethyl)amino]sulfonyl]benzoic acid methyl ester

: 31914-88-2
5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

Guidance literature:: 4-chloro-2-[(2-furanylmethyl)amino]-5-[[(phenylmethyl)amino]sulfonyl]benzoic acid methyl ester; With lithium hydroxide; water; In methanol; at 25 ℃; for 24h; under 760.051 Torr;

With hydrogenchloride; In methanol; water; at 25 ℃; under 760.051 Torr;

Reference yield: 57.0%

: 617-89-0
furan-2-ylmethanamine

: C₁₄H₁₁ClFNO₄S

: 31914-88-2
5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

Guidance literature:: With triethylamine; In ethylene glycol; at 130 ℃; for 16h;
DOI:10.1016/j.ejmech.2021.113565

Reference yield:

: 446-30-0
4-chloro-2-fluorobenzoic acid

: 31914-88-2
5-(N-benzylsulfamoyl)-4-chloro-2-((furan-2-ylmethyl)amino)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / 5 h / 0 - 140 °C

2: triethylamine / tetrahydrofuran / 0 - 20 °C

3: triethylamine / ethylene glycol / 16 h / 130 °C

With chlorosulfonic acid; triethylamine; In tetrahydrofuran; ethylene glycol;
DOI:10.1016/j.ejmech.2021.113565