2,2-dimethyl-3-oxocyclopentyl benzoate

Base Information

Chemical Name:2,2-dimethyl-3-oxocyclopentyl benzoate
CAS No.:1333210-93-7
Molecular Formula:C₁₄H₁₆O₃
Molecular Weight:232.279
Hs Code.:

Synonyms:2,2-dimethyl-3-oxocyclopentyl benzoate

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Chemical Property of 2,2-dimethyl-3-oxocyclopentyl benzoate

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Technology Process of 2,2-dimethyl-3-oxocyclopentyl benzoate

There total 3 articles about 2,2-dimethyl-3-oxocyclopentyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3-hydroxy-2,2-dimethylcyclopentyl benzoate

: 1333210-93-7
2,2-dimethyl-3-oxocyclopentyl benzoate

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; at 20 ℃; for 1.33333h; Inert atmosphere;
DOI:10.1021/ol202147r

Reference yield:

: 3883-58-7
2,2-dimethylcyclopentane-1,3-dione

: 1333210-93-7
2,2-dimethyl-3-oxocyclopentyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / tetrahydrofuran; water / 2.5 h / 20 °C

2: pyridine / 3 h / 20 °C

3: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.33 h / 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol202147r

Reference yield:

: 1333211-04-3
(1R,3S)-2,2-dimethylcyclopentane-1,3-diol

: 1333210-93-7
2,2-dimethyl-3-oxocyclopentyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 3 h / 20 °C

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1.33 h / 20 °C / Inert atmosphere

With pyridine; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane;
DOI:10.1021/ol202147r