3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine

Base Information

• Chemical Name: 3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine
• CAS No.: 853581-67-6
• Molecular Formula: C₁₇H₂₃N₃O₄
• Molecular Weight: 333.387

Synonyms:3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine

Chemical Property of 3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine

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Technology Process of 3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine

There total 1 articles about 3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydroisoxazole-5-carbonitrile (853581-66-5) → 3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine (853581-67-6)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; Heating / reflux;

Reference yield: 50.0%

3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine (853581-67-6) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → 3-[3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydroisoxazol-5-yl]-4H-[1,2,4]oxadiazole-5-thione (853581-70-1)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃;

Reference yield: 46.0%

3-(3-cyclopentyloxy-4-methoxyphenyl)-N-hydroxy-5-methyl-4,5-dihydroisoxazole-5-carboxamidine (853581-67-6) + acetic anhydride (108-24-7) → acetic acid (Z)-2-amino-2-{3-[3-(cyclopentyloxy)-4-methoxyphenyl]-5-methyl-4,5-dihydroisoxazol-5-yl}vinyl ester

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

upstream raw materials:

3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydroisoxazole-5-carbonitrile

Downstream raw materials:

5-tert-butyl-3-[3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydro-isoxazol-5-yl]-[1,2,4]oxadiazole

3-[3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydroisoxazol-5-yl]-4H-[1,2,4]oxadiazole-5-thione

3-[3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydroisoxazol-5-yl]-4H-[1,2,4]thiadiazol-5-one

3-[3-(3-cyclopentyloxy-4-methoxyphenyl)-5-methyl-4,5-dihydro-isoxazol-5-yl]-4H-[1,2,4]oxadiazol-5-one

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