(E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

Base Information

Chemical Name:(E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime
CAS No.:1404220-64-9
Molecular Formula:C₁₇H₂₀N₂O₄S
Molecular Weight:348.423
Hs Code.:

Synonyms:(E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

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Technology Process of (E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

There total 2 articles about (E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 85862-86-8
1-azido-4-(methylsulfonyl)benzene

: 80965-21-5
(E)-1-(4-methoxyphenyl)ethan-1-one O-methyl oxime

: 1404220-64-9
(E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; In 1,2-dichloro-ethane; at 85 ℃; for 24h;
DOI:10.1002/anie.201205723

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1404220-64-9
(E)-1-[4-methoxy-2-(4-(methylsulfonyl)phenylamino)phenyl]ethanone O-methyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / ethanol; water / 12 h / 80 °C

2: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 85 °C

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium acetate; In ethanol; water; 1,2-dichloro-ethane;
DOI:10.1002/anie.201205723