N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine

Base Information

• Chemical Name: N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine
• CAS No.: 1253796-06-3
• Molecular Formula: C₃₀H₄₇N₃O₇Si₂
• Molecular Weight: 617.89

Synonyms:N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine

Chemical Property of N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine

Chemical Property:

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Technology Process of N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine

There total 1 articles about N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N4-hydroxycytidine (1253796-04-1) + benzoic acid anhydride (93-97-0) → N4-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N4-hydroxycytidine (1253796-06-3)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1055/s-0030-1258170

Reference yield: 97.0%

N4-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N4-hydroxycytidine (1253796-06-3) → N4-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-N4-hydroxycytidine (1253796-08-5)

Guidance literature:

With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0030-1258170

upstream raw materials:

2'-O-[(tert-butyl)dimethylsilyl]-3',5'-O-(di-tert-butylsilylene)-N₄-hydroxycytidine

benzoic acid anhydride

Downstream raw materials:

N₄-benzoyl-2'-O-[(tert-butyl)dimethylsilyl]-N₄-hydroxycytidine

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