N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

Base Information

Chemical Name:N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam
CAS No.:214466-02-1
Molecular Formula:C₂₂H₂₉NO₅S
Molecular Weight:419.542
Hs Code.:

Synonyms:N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

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Chemical Property of N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

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Technology Process of N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

There total 1 articles about N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 94594-90-8,124224-04-0
(2R)-bornane-10,2-sultam

: (E)-3-(3,5-Dimethoxy-phenyl)-2-methyl-acryloyl chloride

: 214466-02-1
N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

Guidance literature:: (2R)-bornane-10,2-sultam; With sodium hydride; In toluene; at 0 - 20 ℃; for 1h;

(E)-3-(3,5-Dimethoxy-phenyl)-2-methyl-acryloyl chloride; In toluene; at 0 - 20 ℃; for 3h;
DOI:10.1016/S0040-4020(01)00729-3

Reference yield: 85.0%

: 214466-02-1
N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

: 214466-03-2
(2S,3S)-3-(3,5-Dimethoxy-phenyl)-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-2-methyl-butan-1-one

Guidance literature:: In toluene; at -40 ℃;
DOI:10.1016/S0960-894X(98)00385-0

Reference yield:

: 214466-02-1
N-[(E)-2-methyl-3-{3,5-dimethoxyphenyl}-2-propenoyl]-bornane-10,2-sultam

: 199388-20-0
3'S-(3,5-dimethoxyphenyl)-2'S-methyl-1-butanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: CuI / toluene; diethyl ether / 1 h / -40 °C

1.2: 85 percent / toluene / -78 - -40 °C

2.1: 100 percent / aq. LiOH / tetrahydrofuran / 96 h / 60 °C

3.1: 90 percent / LiAlH₄ / tetrahydrofuran / 16 h / 0 - 20 °C

With lithium hydroxide; copper(l) iodide; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1016/S0040-4020(01)00729-3