2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

Base Information

Chemical Name:2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose
CAS No.:454474-75-0
Molecular Formula:C₁₇H₂₄O₆
Molecular Weight:324.374
Hs Code.:

Synonyms:2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

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Chemical Property of 2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

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Technology Process of 2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

There total 5 articles about 2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 454475-03-7
(3aR,4S,6aR)-4-[(S)-1-(4-Methoxy-benzyloxy)-ethyl]-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxole

: 454474-75-0
2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

Guidance literature:: With N-Bromosuccinimide; In tetrahydrofuran; water; at 0 ℃; Yield given;
DOI:10.1016/S0040-4039(98)02440-X

Reference yield:

: 454474-74-9
phenyl 2,3-O-isopropylidene-1-thio-L-rhamnofuranoside

: 454474-75-0
2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: NaH; n-Bu₄NI / dimethylformamide; various solvent(s) / 19 h / 0 °C

2: 5.53 g / N-bromosuccinimide / tetrahydrofuran; H₂O / 0.33 h / 0 °C

With N-Bromosuccinimide; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jo020211h

Reference yield:

: phenyl 5-O-acetyl-2,3-O-isopropylidene-1-thio-L-rhamnofuranoside

: 454474-75-0
2,3-O-isopropylidene-5-O-p-methoxybenzyl-L-rhamnofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / sodium methoxide / methanol / 16 h / 20 °C

2: NaH; n-Bu₄NI / dimethylformamide; various solvent(s) / 19 h / 0 °C

3: 5.53 g / N-bromosuccinimide / tetrahydrofuran; H₂O / 0.33 h / 0 °C

With N-Bromosuccinimide; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo020211h