(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

Base Information

Chemical Name:(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester
CAS No.:47820-69-9
Molecular Formula:C₂₉H₄₀N₄O₇
Molecular Weight:556.659
Hs Code.:

Synonyms:(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

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Chemical Property of (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

There total 1 articles about (S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59658-28-5
Z(OMe)-Lys(Z)-Lys(Z)-OMe

: 47820-69-9
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

Guidance literature:: With methoxybenzene; trifluoroacetic acid;
DOI:10.1248/cpb.36.3857

Reference yield: 90.0%

: 47820-69-9
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

: 119089-48-4
[(S)-1-((S)-1-Azidocarbonyl-3-methanesulfinyl-propylcarbamoyl)-ethyl]-carbamic acid 4-methoxy-benzyl ester

: Z(OMe)-Ala-Met(O)-Lys(Z)-Lys(Z)-OMe

Guidance literature:: With TEA; In N,N-dimethyl-formamide; at 4 ℃; for 24h;
DOI:10.1248/cpb.36.3857

Reference yield:

: 47820-69-9
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

: 119178-11-9
((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / TEA / dimethylformamide / 24 h / 4 °C

2: 73 percent / 80percent NH₂NH₂*H₂O / dimethylformamide; methanol / 24 h / Ambient temperature

With TEA; hydrazine hydrate; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3857