((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

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Chemical Name:((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester
CAS No.:119178-11-9
Molecular Formula:C₄₅H₅₉N₉O₁₂S
Molecular Weight:950.083
Hs Code.:

((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

Synonyms:((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

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Chemical Property of ((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

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Technology Process of ((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

There total 8 articles about ((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 47820-69-9
(S)-2-((S)-2-Amino-6-benzyloxycarbonylamino-hexanoylamino)-6-benzyloxycarbonylamino-hexanoic acid methyl ester

: 119178-11-9
((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / TEA / dimethylformamide / 24 h / 4 °C

2: 73 percent / 80percent NH₂NH₂*H₂O / dimethylformamide; methanol / 24 h / Ambient temperature

With TEA; hydrazine hydrate; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3857

Reference yield:

: 59658-28-5
Z(OMe)-Lys(Z)-Lys(Z)-OMe

: 119178-11-9
((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: TFA, anisole

2: 90 percent / TEA / dimethylformamide / 24 h / 4 °C

3: 73 percent / 80percent NH₂NH₂*H₂O / dimethylformamide; methanol / 24 h / Ambient temperature

With TEA; hydrazine hydrate; methoxybenzene; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3857

Reference yield:

: 62074-69-5
Z(OMe)-Ala-Met-OMe

: 119178-11-9
((S)-5-((S)-1-Azidocarbonyl-5-benzyloxycarbonylamino-pentylcarbamoyl)-5-{(S)-4-methanesulfinyl-2-[(S)-2-(4-methoxy-benzyloxycarbonylamino)-propionylamino]-butyrylamino}-pentyl)-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / NaIO₄ / H₂O; methanol / 20 h / Ambient temperature

2: 75 percent / 80percent NH₂NH₂*H₂O / methanol / 18 h / Ambient temperature

4: 90 percent / TEA / dimethylformamide / 24 h / 4 °C

5: 73 percent / 80percent NH₂NH₂*H₂O / dimethylformamide; methanol / 24 h / Ambient temperature

With sodium periodate; TEA; hydrazine hydrate; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3857