1--2,4-cyclohexadiene

Base Information

Chemical Name:1--2,4-cyclohexadiene
CAS No.:106093-66-7
Molecular Formula:C₁₄H₂₁NO₅
Molecular Weight:283.324
Hs Code.:

1-<bis(methoxycarbonyl)((dimethylamino)methyl)methoxy>-2,4-cyclohexadiene

Synonyms:1--2,4-cyclohexadiene

Suppliers and Price of 1--2,4-cyclohexadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1--2,4-cyclohexadiene

Chemical Property:

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Technology Process of 1--2,4-cyclohexadiene

There total 3 articles about 1--2,4-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 33797-51-2
eschenmoser's salt

: 106093-52-1
1--2,4-cyclohexadiene

: 106093-66-7
1--2,4-cyclohexadiene

Guidance literature:: With triethylamine; In dichloromethane; for 5h;
DOI:10.1021/ja00238a029

Reference yield:

: 6773-29-1
dimethyl diazomalonate

: 106093-66-7
1--2,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 36.5 percent / rhodium acetate dimer / benzene / 2 h / 65 °C

2: 66 percent / Et₃N / CH₂Cl₂ / 5 h

With dirhodium tetraacetate; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ja00238a029

Reference yield:

: 108-59-8
malonic acid dimethyl ester

: 106093-66-7
1--2,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / p-TsN₃, Et₃N / benzene / 15 h / Ambient temperature

2: 36.5 percent / rhodium acetate dimer / benzene / 2 h / 65 °C

3: 66 percent / Et₃N / CH₂Cl₂ / 5 h

With dirhodium tetraacetate; 4-toluenesulfonyl azide; triethylamine; In dichloromethane; benzene;
DOI:10.1021/ja00238a029