phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

Base Information

Chemical Name:phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate
CAS No.:1300090-44-1
Molecular Formula:C₃₀H₂₄ClN₅O₅
Molecular Weight:570.004
Hs Code.:

Synonyms:phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

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Chemical Property of phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

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Technology Process of phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

There total 6 articles about phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91713-54-1
[2-amino-5-(methyloxy)phenyl](4-chlorophenyl)methanone

: 124676-19-3
2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine

: 1300090-44-1
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: 2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at -10 - 0 ℃; for 3.08333h;

[2-amino-5-(methyloxy)phenyl](4-chlorophenyl)methanone; With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃; for 48h;

Reference yield:

: 91713-54-1
[2-amino-5-(methyloxy)phenyl](4-chlorophenyl)methanone

: 517874-18-9
(Benzotriazol-1-yl-chlorocarbonyl-methyl)-carbamic acid benzyl ester

: 1300090-44-1
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃; for 48h;

Reference yield:

: 873-77-8
(4-chlorphenyl)magnesium bromide

: 1300090-44-1
phenylmethyl (1-(1H-1,2,3-benzotriazol-1-yl)-2-{[2-[(4-chlorophenyl)carbonyl]-4-(methyloxy)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene; diethyl ether / 1 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: 4-methyl-morpholine / tetrahydrofuran / 48 h / 0 - 20 °C

With 4-methyl-morpholine; In tetrahydrofuran; diethyl ether; toluene;