Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

Base Information

Chemical Name:Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester
CAS No.:95687-98-2
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

Suppliers and Price of Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

There total 4 articles about Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 95687-98-2
Benzoic acid (1R,3R,6S)-3-benzyloxycarbonylamino-6-hydroxy-cycloheptyl ester

Guidance literature:: With sodium carbonate; In chloroform; at 0 - 25 ℃;
DOI:10.1016/S0040-4039(01)91127-X

Reference yield:

: 59171-91-4
cyclohepta-3,5-dien-1-yl benzoate

: 95687-98-2
all-cis-3-(benzoyloxy)-5-(<(benzyloxy)carbonyl>amino)-cycloheptanol

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / ethanol; CCl₄ / 1.) -20 deg C, 5 h, 2.) -10 deg C, 14 d

2: 98 percent / H₂ / 5percent Pd/C / methanol / 7 h

3: Na₂CO₃ / 1.) chloroform, water, 0 deg C, 30 min, 2.) RT, 2h

With hydrogen; sodium carbonate; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol;
DOI:10.1021/jo00211a006

Reference yield:

: 95687-89-1,95782-70-0
exo-3-(benzoyloxy)-8-oxa-9-azabicyclo<3.2.2.>-non-6-ene hydrochloride

: 95687-98-2
all-cis-3-(benzoyloxy)-5-(<(benzyloxy)carbonyl>amino)-cycloheptanol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂ / 5percent Pd/C / methanol / 7 h

2: Na₂CO₃ / 1.) chloroform, water, 0 deg C, 30 min, 2.) RT, 2h

With hydrogen; sodium carbonate; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00211a006