5-BROMO-4-METHOXY-1H-INDAZOLE

Base Information

• Chemical Name: 5-BROMO-4-METHOXY-1H-INDAZOLE
• CAS No.: 850363-67-6
• Molecular Formula: C₈H₇BrN₂O
• Molecular Weight: 227.06
• Hs Code.: 2933990090
• Mol file: 850363-67-6.mol

Synonyms:5-Bromo-4-methoxy-1H-indazole;5-bromo-4-methoxy-1H-indazole;5-Bromo-4-Methoxy-1H-Indazole;

Chemical Property of 5-BROMO-4-METHOXY-1H-INDAZOLE

Chemical Property:

• Vapor Pressure: 3.78E-05mmHg at 25°C
• Refractive Index: 1.677
• Boiling Point: 363.4 °C at 760 mmHg
• Flash Point: 173.6 °C
• PSA: 37.91000
• Density: 1.678 g/cm³
• LogP: 2.33400
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-4-methoxy-1H-indazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BROMO-4-METHOXY-1H-INDAZOLE

There total 7 articles about 5-BROMO-4-METHOXY-1H-INDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.9%

1-(5-bromo-4-methoxy-1H-indazol-1-yl)ethanone → 5-bromo-4-methoxy-1H-indazole (850363-67-6)

Guidance literature:

With ammonium hydroxide; In methanol; for 1h;

Reference yield: 41.0%

3-bromo-6-fluoro-2-methoxybenzaldehyde (473416-74-9) → 5-bromo-4-methoxy-1H-indazole (850363-67-6)

Guidance literature:

With hydrazine hydrate; In dimethyl sulfoxide; at 130 ℃; for 16h;

Reference yield:

C9H9BrFNO3 → 5-bromo-4-methoxy-1H-indazole (850363-67-6)

Guidance literature:

With hydrazine; In 1,2-dimethoxyethane; at 100 ℃; for 15h;

upstream raw materials:

3-bromo-6-fluoro-2-methoxybenzaldehyde

1-bromo-4-fluoro-2-methoxybenzene

N-methoxylamine hydrochloride

4-methoxy-1H-indazole

Downstream raw materials:

5-bromo-1-(3-fluoro-4-hydroxyphenyl)-1H-indazol-4-ol

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