Fmoc-PheΨ(NHCO)Gly-OBu

Base Information

Chemical Name:Fmoc-PheΨ(NHCO)Gly-OBu
CAS No.:872721-00-1
Molecular Formula:C₃₀H₃₂N₂O₅
Molecular Weight:500.594
Hs Code.:

Synonyms:Fmoc-PheΨ(NHCO)Gly-OBu

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Chemical Property of Fmoc-PheΨ(NHCO)Gly-OBu

Chemical Property:

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Technology Process of Fmoc-PheΨ(NHCO)Gly-OBu

There total 4 articles about Fmoc-PheΨ(NHCO)Gly-OBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₂N₂O₃

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 872721-00-1
Fmoc-PheΨ(NHCO)Gly-OBu

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; for 15h;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 872721-00-1
Fmoc-PheΨ(NHCO)Gly-OBu

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-hydroxy-5-norbornene-2,3-dicarboxylic acid imide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 4 h / 0 - 35 °C

1.2: 4 h / 0 °C

2.1: bis-[(trifluoroacetoxy)iodo]benzene; pyridine / water; acetonitrile / 15 h / 0 - 35 °C

2.2: 15 h / 0 - 35 °C

3.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

4.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 15 h

With pyridine; palladium 10% on activated carbon; N-hydroxy-5-norbornene-2,3-dicarboxylic acid imide; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; In methanol; water; acetonitrile;

Reference yield:

: 5241-56-5,17324-88-8,53562-23-5,4801-80-3
benzyl [(2S)-1-amino-1-oxo-3-phenylpropan-2-yl]carbamate

: 872721-00-1
Fmoc-PheΨ(NHCO)Gly-OBu

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-[(trifluoroacetoxy)iodo]benzene; pyridine / water; acetonitrile / 15 h / 0 - 35 °C

1.2: 15 h / 0 - 35 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 15 h

With pyridine; palladium 10% on activated carbon; hydrogen; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; In methanol; water; acetonitrile;