N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

Base Information

Chemical Name:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline
CAS No.:1235481-52-3
Molecular Formula:C₂₃H₂₂Br₂N₂O₂
Molecular Weight:518.248
Hs Code.:

Synonyms:N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

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Chemical Property of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

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Technology Process of N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

There total 13 articles about N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 313268-18-7
1-(3,6-dibromo-9H-carbazol-9-yl)-3-((3-methoxyphenyl)amino)propan-2-ol

: 74-88-4
methyl iodide

: 1235481-52-3
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

Guidance literature:: 1-(3,6-dibromo-9H-carbazol-9-yl)-3-((3-methoxyphenyl)amino)propan-2-ol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1.16667h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja108211m

Reference yield:

: C₃₀H₂₈Br₂N₂O₂

: 1235481-52-3
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

Guidance literature:: With diphenyl sulfide; palladium on activated carbon; hydrogen; In tetrahydrofuran; ethanol; at 20 ℃; for 17h;
DOI:10.1016/j.bmc.2013.08.066

Reference yield:

: 6825-20-3
3,6-dibromo-9H-carbazole

: 1235481-52-3
N-(3-(3,6-dibromo-9H-carbazol-9-yl)-2-methoxypropyl)-3-methoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

1.2: 20 °C

2.1: bismuth(III) chloride / cyclohexane / Reflux

3.1: sodium hydride / N,N-dimethyl-formamide / 1.17 h / 20 °C

3.2: 20 °C

With bismuth(III) chloride; sodium hydride; potassium hydroxide; In cyclohexane; N,N-dimethyl-formamide;
DOI:10.1021/ja108211m