C₇₄H₆₀O₁₀P₂

Base Information

Chemical Name:C₇₄H₆₀O₁₀P₂
CAS No.:627545-46-4
Molecular Formula:C₇₄H₆₀O₁₀P₂
Molecular Weight:1171.23
Hs Code.:

C<sub>74</sub>H<sub>60</sub>O<sub>10</sub>P<sub>2</sub>

Synonyms:C₇₄H₆₀O₁₀P₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₇₄H₆₀O₁₀P₂

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Technology Process of C₇₄H₆₀O₁₀P₂

There total 4 articles about C₇₄H₆₀O₁₀P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 797032-45-2,627545-43-1
C₅₀H₄₀Br₂O₈

: 1499-21-4
Diphenylphosphinic chloride

: 627545-46-4
C₇₄H₆₀O₁₀P₂

Guidance literature:: C₅₀H₄₀Br₂O₈; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.666667h;

Diphenylphosphinic chloride; In tetrahydrofuran; hexane; at -78 - 25 ℃; for 10h;
DOI:10.1021/jo035057t

Reference yield:

: 100-39-0
benzyl bromide

: 627545-46-4
C₇₄H₆₀O₁₀P₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / NaH / dimethylformamide / 10 h / 25 °C

2.1: 96 percent / NBS / acetonitrile; CH₂Cl₂ / 2 h / 25 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.67 h / -78 °C

3.2: 62 percent / tetrahydrofuran; hexane / 10 h / -78 - 25 °C

With N-Bromosuccinimide; n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo035057t

Reference yield:

: 310899-19-5,312323-69-6,312323-70-9
C₃₆H₃₀O₈

: 627545-46-4
C₇₄H₆₀O₁₀P₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: 82 percent / NaH / dimethylformamide / 10 h / 25 °C

2.1: 96 percent / NBS / acetonitrile; CH₂Cl₂ / 2 h / 25 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.67 h / -78 °C

3.2: 62 percent / tetrahydrofuran; hexane / 10 h / -78 - 25 °C

With N-Bromosuccinimide; n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo035057t