(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

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Chemical Name:(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol
CAS No.:1443249-98-6
Molecular Formula:C₂₃H₂₁N₃O₂
Molecular Weight:371.439
Hs Code.:

Synonyms:(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

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Chemical Property of (Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

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Technology Process of (Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

There total 5 articles about (Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1443249-97-5
(Z)-5-(4-methoxyphenyl)-N-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylidene)-3-methyl-1H-pyrrol-2-amine

: 1443249-98-6
(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

Guidance literature:: With boron tribromide; In dichloromethane; at -78 ℃; for 3h;
DOI:10.1021/ol401434c

Reference yield:

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 1443249-98-6
(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

Guidance literature:: Multi-step reaction with 5 steps

1: 0.25 h / 0 °C

2: manganese(IV) oxide / diethyl ether / 20 h / 20 °C

3: diethylamine / ethanol / 5 h / Reflux

4: ammonium acetate / methanol / 10 h / Reflux

5: boron tribromide / dichloromethane / 3 h / -78 °C

With manganese(IV) oxide; ammonium acetate; boron tribromide; diethylamine; In methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/ol401434c

Reference yield:

: 97060-29-2
1-(4-methoxyphenyl)-but-2-en-1-one

: 1443249-98-6
(Z)-4-(5-(5-(4-methoxyphenyl)-3-methyl-2H-pyrrol-2-ylideneamino)-4-methyl-1H-pyrrol-2-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: diethylamine / ethanol / 5 h / Reflux

2: ammonium acetate / methanol / 10 h / Reflux

3: boron tribromide / dichloromethane / 3 h / -78 °C

With ammonium acetate; boron tribromide; diethylamine; In methanol; ethanol; dichloromethane;
DOI:10.1021/ol401434c