methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

Base Information

Chemical Name:methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate
CAS No.:101774-01-0
Molecular Formula:C₃₂H₃₄N₂O₉S₂
Molecular Weight:654.762
Hs Code.:

Synonyms:methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

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Chemical Property of methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

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Technology Process of methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

There total 5 articles about methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 103478-10-0
4-(N-benzyloxycarbonyl-L-alanyloxy)-6-dibenzofuranthiol

: 53907-23-6
methyl-N-(tert-butoxycarbonyl)-S-(methoxycarbonylsulfenyl)-L-cysteinate

: 101774-01-0
methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

Guidance literature:: In chloroform; for 0.5h; Ambient temperature;
DOI:10.1021/jo00273a008

Reference yield:

: 101697-56-7
4-(methoxycarbonyldithio)-6-(N-benzyloxycarbonyl-L-alaninyloxy)dibenzofuran

: 101774-01-0
methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / (n-Bu)3P / dioxane; H₂O

2: 90 percent / CHCl₃; various solvent(s) / 0.5 h

With tributylphosphine; In 1,4-dioxane; chloroform; water;
DOI:10.1021/jo00367a013

Reference yield:

: 101697-58-9
4-(methoxycarbonyldithio)-6-hydroxydibenzofuran

: 101774-01-0
methyl N-(tert-butoxycarbonyl)-S-<6-(N-benzyloxycarbonyl-L-alaninyloxy)-4-dibenzofuranylthio>-L-cysteinate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / DCC / 12 h

2: 62 percent / (n-Bu)3P / dioxane; H₂O

3: 90 percent / CHCl₃; various solvent(s) / 0.5 h

With tributylphosphine; dicyclohexyl-carbodiimide; In 1,4-dioxane; chloroform; water;
DOI:10.1021/jo00367a013