N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

Base Information

Chemical Name:N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide
CAS No.:1388233-69-9
Molecular Formula:C₂₁H₉F₁₀NO
Molecular Weight:481.293
Hs Code.:

Synonyms:N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

Chemical Property:

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Technology Process of N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

There total 3 articles about N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1388233-82-6
C₂₀H₁₀F₇NO

: 129946-88-9
Umemoto's reagent

: 1388233-69-9
N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

Guidance literature:: With N-Methylformamide; copper diacetate; palladium diacetate; trifluoroacetic acid; In 1,2-dichloro-ethane; at 130 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja305259n

Reference yield:

: 42498-44-2
3-phenylbenzoyl chloride

: 1388233-69-9
N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / Reflux

2: N-Methylformamide; copper diacetate; palladium diacetate; trifluoroacetic acid / 1,2-dichloro-ethane / 24 h / 130 °C / Inert atmosphere

With N-Methylformamide; copper diacetate; palladium diacetate; trifluoroacetic acid; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja305259n

Reference yield:

: 716-76-7
3-phenylbenzoic acid

: 1388233-69-9
N-(2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)-4-(trifluoromethyl)-[1,1'-biphenyl]-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 20 °C

2: toluene / Reflux

3: N-Methylformamide; copper diacetate; palladium diacetate; trifluoroacetic acid / 1,2-dichloro-ethane / 24 h / 130 °C / Inert atmosphere

With N-Methylformamide; thionyl chloride; copper diacetate; palladium diacetate; trifluoroacetic acid; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/ja305259n