benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

Base Information

Chemical Name:benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate
CAS No.:1579276-55-3
Molecular Formula:C₂₉H₄₈N₂O₉
Molecular Weight:568.708
Hs Code.:

Synonyms:benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

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Chemical Property of benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

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Technology Process of benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

There total 3 articles about benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1579276-38-2
benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

: 1579276-55-3
benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

Guidance literature:: benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate; With hydrogenchloride; water; In tetrahydrofuran; at 30 ℃; for 1h;

bromoacetic acid tert-butyl ester; With triethylamine; In N,N-dimethyl-formamide; for 18h; pH=Ca. 8;

Reference yield:

: 1579276-37-1
tert-butyl (2-(2-((2-(2-hydroxyethoxy)ethyl)amino)ethoxy)ethyl)carbamate

: 1579276-55-3
benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 0 - 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 1 h / 30 °C

2.2: 18 h / pH Ca_. 8

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;

Reference yield:

: 302331-20-0
methanesulfonic acid 2-(2-tert-butoxycarbonylamino-ethoxy)-ethyl ester

: 1579276-55-3
benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetonitrile / 4 h / Heating

2.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 0 - 20 °C

3.1: hydrogenchloride; water / tetrahydrofuran / 1 h / 30 °C

3.2: 18 h / pH Ca_. 8

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; acetonitrile;