benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Base Information

Chemical Name:benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate
CAS No.:1579276-38-2
Molecular Formula:C₂₂H₃₆N₂O₇
Molecular Weight:440.537
Hs Code.:

Synonyms:benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Suppliers and Price of benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

There total 2 articles about benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1579276-37-1
tert-butyl (2-(2-((2-(2-hydroxyethoxy)ethyl)amino)ethoxy)ethyl)carbamate

: 5437-45-6
Benzyl bromoacetate

: 1579276-38-2
benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 - 20 ℃; for 20h;

Reference yield:

: 302331-20-0
methanesulfonic acid 2-(2-tert-butoxycarbonylamino-ethoxy)-ethyl ester

: 1579276-38-2
benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 4 h / Heating

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 h / 0 - 20 °C

With N-ethyl-N,N-diisopropylamine; In acetonitrile;

Reference yield: 59.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1579276-38-2
benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate

: 1579276-55-3
benzyl 2-[2-[2-(bis(2-(tert-butoxy)-2-oxoethyl)amino)ethoxy]ethyl-[2-(2-hydroxyethoxy)ethyl]amino]acetate

Guidance literature:: benzyl 11-(2-(2-hydroxyethoxy)ethyl)-2,2-dimethyl-4-oxo-3,8-dioxa-5,11-diazatridecan-13-oate; With hydrogenchloride; water; In tetrahydrofuran; at 30 ℃; for 1h;

bromoacetic acid tert-butyl ester; With triethylamine; In N,N-dimethyl-formamide; for 18h; pH=Ca. 8;