N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

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Chemical Name:N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine
CAS No.:442852-10-0
Molecular Formula:C₂₄H₄₅NO₈
Molecular Weight:475.623
Hs Code.:

Synonyms:N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

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Chemical Property of N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

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Technology Process of N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

There total 7 articles about N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 442851-98-1
N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

: 442852-10-0
N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Guidance literature:: With acetic acid; In water; at 60 ℃; for 2h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 442852-10-0
N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 2.5 h / 25 °C

2: AcOH / H₂O / 0.5 h / 60 °C

3: 164 mg / p-TsOH*H₂O / dimethylformamide / 5.5 h / 45 °C

4: 99 percent / N,N-diiisopropylethylamine / 1,2-dichloro-ethane / 3 h / 60 °C

5: AcOH / H₂O / 2 h / 60 °C

With toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00005-6

Reference yield:

: 177898-40-7
N-octyl-2,3:4,6-di-O-isopropylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

: 442852-10-0
N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 2.5 h / 25 °C

2: AcOH / H₂O / 0.5 h / 60 °C

3: 164 mg / p-TsOH*H₂O / dimethylformamide / 5.5 h / 45 °C

4: 99 percent / N,N-diiisopropylethylamine / 1,2-dichloro-ethane / 3 h / 60 °C

5: AcOH / H₂O / 2 h / 60 °C

With toluene-4-sulfonic acid; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00005-6