N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Base Information

• Chemical Name: N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine
• CAS No.: 442852-08-6
• Molecular Formula: C₂₀H₃₇NO₆
• Molecular Weight: 387.517

Synonyms:N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Chemical Property of N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine

There total 3 articles about N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-octyl-N-tert-butoxycarbonyl-2,3:4,6-di-O-isopropylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine (442851-92-5) → N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine (442852-08-6)

Guidance literature:

With acetic acid; In water; at 60 ℃; for 0.5h;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine (442852-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 2.5 h / 25 °C

2: AcOH / H₂O / 0.5 h / 60 °C

With acetic acid; triethylamine; In dichloromethane; water;

DOI:10.1016/S0968-0896(02)00005-6

Reference yield:

N-octyl-2,3:4,6-di-O-isopropylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine (177898-40-7) → N-octyl-N-tert-butoxycarbonyl-1-deoxy-5a-carba-β-D-xylo-hexo-5(5a)-enopyranosylamine (442852-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / Et₃N / CH₂Cl₂ / 2.5 h / 25 °C

2: AcOH / H₂O / 0.5 h / 60 °C

With acetic acid; triethylamine; In dichloromethane; water;

DOI:10.1016/S0968-0896(02)00005-6

upstream raw materials:

N-octyl-N-tert-butoxycarbonyl-2,3:4,6-di-O-isopropylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

di-tert-butyl dicarbonate

N-octyl-2,3:4,6-di-O-isopropylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

Downstream raw materials:

N-octyl-N-tert-butoxycarbonyl-4,6-O-benzylidene-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

((3aS,4R,9aR,9bS)-2,8-Diphenyl-4,6,9a,9b-tetrahydro-3aH-[1,3]dioxolo[4',5':3,4]benzo[1,2-d][1,3]dioxin-4-yl)-octyl-carbamic acid tert-butyl ester

N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-6-O-tert-butyldimethylsilyl-5a-carba-α-L-arabino-hex-5(5a)-enopyranosylamine

N-octyl-N-tert-butoxycarbonyl-2,3-di-O-methoxymethyl-6-O-tert-butyldimethylsilyl-5a-carba-β-D-xylo-hex-5(5a)-enopyranosylamine

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