2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol

Base Information

• Chemical Name: 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol
• CAS No.: 306776-34-1
• Molecular Formula: C₂₀H₄₀N₂O₂S₂
• Molecular Weight: 404.682

Synonyms:2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol

Chemical Property of 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol

Chemical Property:

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Technology Process of 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol

There total 2 articles about 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.5%

2-[({[({[(2-Hydroxyethyl)amino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)amino]ethan-1-ol (306776-69-2) → 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol (306776-34-1)

Guidance literature:

With sodium tetrahydroborate; formaldehyd; In methanol; water; ethyl acetate;

Reference yield: 88.5%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 2-[({[({[(2-Hydroxyethyl)amino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)amino]ethan-1-ol (306776-69-2) → 2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol (306776-34-1)

Guidance literature:

formaldehyd; 2-[({[({[(2-Hydroxyethyl)amino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)amino]ethan-1-ol; In methanol; water; at 20 ℃; for 12h;

With sodium tetrahydroborate; In methanol; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/jm000178w

Reference yield: 79.0%

2-[({[({[(2-Hydroxyethyl)methylamino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)methylamino]ethan-1-ol (306776-34-1) → 2-{Methyl[(sulfanylcyclohexyl)methyl]amino}ethan-1-ol (306776-38-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/jm000178w

upstream raw materials:

formaldehyd

2-[({[({[(2-Hydroxyethyl)amino]methyl}cyclohexyl)disulfanyl]cyclohexyl}methyl)amino]ethan-1-ol

Downstream raw materials:

2-{Methyl[(sulfanylcyclohexyl)methyl]amino}ethan-1-ol

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