5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

Base Information

Chemical Name:5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide
CAS No.:1421921-85-8
Molecular Formula:C₂₅H₃₀N₄OS
Molecular Weight:434.605
Hs Code.:

Synonyms:5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

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Chemical Property of 5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

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Technology Process of 5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

There total 8 articles about 5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421923-02-5
5-(bromoacetyl)-N,2-dimethylbenzamide

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

: 1421921-85-8
5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

Guidance literature:: In isopropyl alcohol; at 80 ℃; for 1h;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421921-85-8
5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid / 0.5 h / Cooling with ice

2.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

4.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

4.2: 24 h / 20 °C

5.1: isopropyl alcohol / 1 h / 80 °C

With hydrogenchloride; oxalyl dichloride; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate; isopropyl alcohol;

Reference yield:

: 1421922-03-3
(2,5-dimethyl-4-nitrophenyl)acetonitrile

: 1421921-85-8
5-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N,2-dimethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

2.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

3.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

3.2: 24 h / 20 °C

4.1: isopropyl alcohol / 1 h / 80 °C

With hydrogenchloride; oxalyl dichloride; water; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate; isopropyl alcohol;