4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Base Information

Chemical Name:4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide
CAS No.:1312698-82-0
Molecular Formula:C₉H₈BrN₅OS₂
Molecular Weight:346.231
Hs Code.:

Synonyms:4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Suppliers and Price of 4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

There total 5 articles about 4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₄BrN₃OS₂

: 1312698-82-0
4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: With hydrazine hydrate; In toluene; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 887584-46-5
C₈H₆BrN₃OS

: 1312698-82-0
4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

2: hydrazine hydrate / toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; In acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017

Reference yield:

: 106896-49-5
methyl 4-amino-3-bromobenzoate

: 1312698-82-0
4-(2-bromo-4-(5-mercapto-1,3,4-oxadiazol-2-yl)phenyl)thiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrazine hydrate / 1 h / Reflux

2.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 0 °C / Inert atmosphere; Reflux

2.2: pH 4

3.1: sodium hydrogencarbonate / acetone / 0.5 h / 0 - 20 °C

4.1: hydrazine hydrate / toluene / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine hydrate; potassium hydroxide; In ethanol; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.ejmech.2011.04.017