1-[(1,1'-biphenyl)-2-yl]-1H-indazole

Base Information

Chemical Name:1-[(1,1'-biphenyl)-2-yl]-1H-indazole
CAS No.:1078735-62-2
Molecular Formula:C₁₉H₁₄N₂
Molecular Weight:270.334
Hs Code.:

Synonyms:1-[(1,1'-biphenyl)-2-yl]-1H-indazole

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Chemical Property of 1-[(1,1'-biphenyl)-2-yl]-1H-indazole

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Technology Process of 1-[(1,1'-biphenyl)-2-yl]-1H-indazole

There total 3 articles about 1-[(1,1'-biphenyl)-2-yl]-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 108-86-1,52753-63-6
bromobenzene

: 2-(1H-indazol-1-yl)-N-phenylbenzamide

: 1078735-62-2
1-[(1,1'-biphenyl)-2-yl]-1H-indazole

Guidance literature:: With (p-cymene)ruthenium(II) chloride; mesitylenecarboxylic acid; potassium carbonate; In o-xylene; at 120 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201701231

Reference yield: 70.0%

: 108-86-1,52753-63-6
bromobenzene

: 7788-69-4
1-phenyl-1H-indazole

: 1078735-62-2
1-[(1,1'-biphenyl)-2-yl]-1H-indazole

Guidance literature:: With C₆Cl₂Ru; potassium carbonate; triphenylphosphine; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 20h; regioselective reaction; Inert atmosphere;
DOI:10.1246/cl.2008.994

Reference yield:

: 7788-69-4
1-phenyl-1H-indazole

: 2996-92-1,46143-12-8
phenyl trimethylsiloxane

: 1078735-62-2
1-[(1,1'-biphenyl)-2-yl]-1H-indazole

: C₂₅H₁₈N₂

Guidance literature:: With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; copper diacetate; silver fluoride; silver(I) triflimide; In 2,2,2-trifluoroethanol; at 30 ℃; for 1h; Overall yield = 94 percent; Overall yield = 28 mg; regioselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1039/d0ob01212b