(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

Base Information

Chemical Name:(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester
CAS No.:421556-68-5
Molecular Formula:C₂₅H₂₄INO₅
Molecular Weight:545.374
Hs Code.:

Synonyms:(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

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Chemical Property of (S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

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Technology Process of (S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

There total 8 articles about (S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 119140-66-8
N-Cbz-O-benzyl-L-tyrosine methyl ester

: 421556-68-5
(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

Guidance literature:: With iodine; silver sulfate; In methanol; at 20 ℃; for 2h;
DOI:10.1021/ja049821k

Reference yield: 97.0%

: 100-39-0
benzyl bromide

: 79677-60-4
(S)-N-benzyloxycarbonyl-3-(4-hydroxy-3-iodophenyl)alanine methyl ester

: 421556-68-5
(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetone; at 56 ℃; for 18h; Inert atmosphere;
DOI:10.1002/chem.201601605

Reference yield:

: 13512-31-7
N-(benzyloxycarbonyl)-L-tyrosine methyl ester

: 421556-68-5
(S)-N-benzyloxycarbonyl-3-(4-benzyloxy-3-iodophenyl)alanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CsCO₃ / acetone / 4 h

2: 100 percent / I₂; Ag₂SO₄ / methanol / 2 h / 20 °C

With iodine; silver sulfate; In methanol; acetone;
DOI:10.1021/ja049821k