2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide

Base Information

• Chemical Name: 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide
• CAS No.: 290325-99-4
• Molecular Formula: C₁₆H₁₉N₅O₈S₂
• Molecular Weight: 473.488

Synonyms:2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide

Chemical Property of 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide

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Technology Process of 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide

There total 1 articles about 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

2-Nitrobenzenesulfonyl chloride (1694-92-4) + 3-azapentane-1,5-diamine (111-40-0,98824-35-2) → 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide (290325-99-4)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/acs.bioconjchem.7b00311

Reference yield: 100.0%

bromoacetic acid tert-butyl ester (5292-43-3) + 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide (290325-99-4) → di-tert-butyl 2,2'-((((2-(tert-butoxy)-2-oxoethyl)azanediyl)bis(ethane-2,1-diyl)) bis((phenylsulfonyl)azanediyl))diacetate

Guidance literature:

With potassium carbonate; In acetonitrile; for 2h; Reflux;

DOI:10.1016/j.tetlet.2008.07.160

Reference yield: 98.0%

tert-Butyl acrylate (1663-39-4,25232-27-3) + 2-nitro-[N-(2{2[(2-nitrophenyl)sulfonylamino]ethylamino})ethyl]benzenesulfonamide (290325-99-4) → 4-(2-(tert-butoxycarbonyl)ethyl)-1,7-bis(2-nitrophenylsulfonyl)-1,4,7-triazaheptane (353246-04-5)

Guidance literature:

In methanol; Heating;

DOI:10.1016/S0040-4020(01)00328-3

upstream raw materials:

2-Nitrobenzenesulfonyl chloride

3-azapentane-1,5-diamine

Downstream raw materials:

4-(2-(tert-butoxycarbonyl)ethyl)-1,7-bis(2-nitrophenylsulfonyl)-1,4,7-triazaheptane

4-((tert-butoxycarbonyl)methyl)-1,7-bis(2-nitrophenylsulfonyl)-1,4,7-triazaheptane

3-(tert-butoxycarbonyl)-N¹,N⁵-bis(2-nitrophenylsulfonyl)-3-azapentane-1,5-diamine

tert-butyl 3,9-bis(2-nitrophenylsulfonyl)-3,6,9,15-tetraazabicyclo[9.3.1]pentadecane-1⁽¹⁵⁾,11,13-triene-6-carbamate

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