biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

Base Information

Chemical Name:biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester
CAS No.:1205681-42-0
Molecular Formula:C₂₈H₃₃N₃O₂
Molecular Weight:443.589
Hs Code.:

Synonyms:biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

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Chemical Property of biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

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Technology Process of biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

There total 1 articles about biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1205681-41-9
biphenyl-2-yl-carbamic acid 1-(2-{4-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethyl]-phenyl}-ethyl)-piperidin-4-yl ester

: 1205681-42-0
biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

Guidance literature:: With hydrazine hydrate; In ethanol; at 90 ℃; for 3h;

Reference yield: 95.0%

: 1205681-42-0
biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

: 65145-13-3
2-fluoro-4-hydroxybenzoic acid

: 1205681-06-6
biphenyl-2-yl-carbamic acid 1-(2-{4-[2-(2-fluoro-4-hydroxy-benzoylamino)-ethyl]-phenyl}-ethyl)-piperidin-4-yl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;

Reference yield: 67.0%

: 1205681-42-0
biphenyl-2-yl-carbamic acid 1-{2-[4-(2-amino-ethyl)-phenyl]-ethyl}-piperidin-4-yl ester

: 621-37-4
m-hydroxyphenylacetic acid

: 1205681-09-9
biphenyl-2-yl-carbamic acid 1-[2-(4-{2-[2-(3-hydroxy-phenyl)-acetylamino]-ethyl}-phenyl)-ethyl]-piperidin-4-yl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 22h; Product distribution / selectivity;