aglycone of dilaspirolactone

Base Information

Chemical Name:aglycone of dilaspirolactone
CAS No.:113119-31-6
Molecular Formula:C₁₅H₁₄O₈
Molecular Weight:322.271
Hs Code.:

Synonyms:aglycone of dilaspirolactone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of aglycone of dilaspirolactone

Chemical Property:

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Technology Process of aglycone of dilaspirolactone

There total 3 articles about aglycone of dilaspirolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 113119-30-5
methyl 3-hydroxy-3-(p-hydroxyphenyl)propionate

: 50-81-7,98966-42-8
ascorbic acid

: 113119-31-6
aglycone of dilaspirolactone

: 113119-34-9,113216-06-1
(S)-3-(4-Hydroxy-phenyl)-3-((3S,3aS,6S,6aR)-3,3a,6-trihydroxy-2-oxo-hexahydro-furo[3,2-b]furan-3-yl)-propionic acid methyl ester

Guidance literature:: In water; at 50 ℃; for 72h;
DOI:10.1021/jo00242a037

Reference yield:

: 1012-12-0
4-(trimethylsiloxy)benzaldehyde

: 113119-31-6
aglycone of dilaspirolactone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA, 3.) NH₄Cl/H₂O / 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, -78 deg C, 1 h, 3.) room temp., THF, hexane, 6 h

2: 46 percent / H₂O / 72 h / 50 °C

With water; ammonium chloride; lithium diisopropyl amide; In water;
DOI:10.1021/jo00242a037