7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione

Base Information

• Chemical Name: 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione
• CAS No.: 181777-14-0
• Molecular Formula: C₂₀H₁₆O₃
• Molecular Weight: 304.345

Synonyms:7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione

Chemical Property of 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione

Chemical Property:

Purity/Quality:

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Technology Process of 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione

There total 3 articles about 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-1H-benzotriazole-4,7-dione (24720-89-6) → 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione (181777-14-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 20 percent / Pb(OAc)4 / CH₂Cl₂ / 0 °C

2: CHCl₃ / 168 h / -10 °C

With lead(IV) acetate; In dichloromethane; chloroform;

DOI:10.3987/com-96-7500

Reference yield:

1-amino-1H-benzotriazole-4,7-diol (26002-64-2) → 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione (181777-14-0)

Guidance literature:

Multi-step reaction with 3 steps

1: AgO, Na₂SO₄ / tetrahydrofuran

2: 20 percent / Pb(OAc)4 / CH₂Cl₂ / 0 °C

3: CHCl₃ / 168 h / -10 °C

With lead(IV) acetate; silver(II) oxide; sodium sulfate; In tetrahydrofuran; dichloromethane; chloroform;

DOI:10.3987/com-96-7500

Reference yield:

buta-1,3-diene (106-99-0,130983-70-9,29406-96-0,9003-17-2) + 2-phenyl-p-benzoquinono[b]oxepine (181776-93-2) → 7-Phenyl-1,4,4a,11a-tetrahydro-6-oxa-cyclohepta[b]naphthalene-5,11-dione (181777-14-0)

Guidance literature:

In chloroform; at -10 ℃; for 168h; Yield given;

DOI:10.3987/com-96-7500

upstream raw materials:

buta-1,3-diene

2-phenyl-p-benzoquinono[b]oxepine

1-amino-1H-benzotriazole-4,7-dione

1-amino-1H-benzotriazole-4,7-diol

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