(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol

Base Information

• Chemical Name: (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol
• CAS No.: 654068-92-5
• Molecular Formula: C₂₃H₃₂O₄SSi
• Molecular Weight: 432.656

Synonyms:(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol

Chemical Property of (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol

Chemical Property:

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Technology Process of (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol

There total 2 articles about (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) + (2Z)-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-ene-1,4-diol (179174-76-6) → (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol (654068-92-5)

Guidance literature:

With 1H-imidazole; In tetrahydrofuran; dichloromethane; at -78 - 20 ℃; for 0.5h;

Reference yield:

1H-imidazole (288-32-4) + tert-butyldimethylsilyl chloride (18162-48-6) + (2Z)-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-ene-1,4-diol (179174-76-6) → (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol (654068-92-5)

Guidance literature:

In tetrahydrofuran; dichloromethane;

Reference yield:

(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-ol (654068-92-5) + 6-bromohexanoyl chloride (22809-37-6) → C29H41BrO5SSi

Guidance literature:

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 20 ℃; for 1.5h;

upstream raw materials:

tert-butyldimethylsilyl chloride

(2Z)-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-ene-1,4-diol

1H-imidazole

Downstream raw materials:

6-bromohexyl(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-yl carbonate

(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-2-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-enyl acetate

2,3-bis(nitrooxy)propyl (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-yl carbonate

4,5-bis(nitrooxy)pentyl (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-[4-(methylsulfonyl)phenyl]-3-phenylbut-2-en-1-yl carbonate

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