ethyl oxalate α-propylbenzylidenehydrazide

Base Information

• Chemical Name: ethyl oxalate α-propylbenzylidenehydrazide
• CAS No.: 84408-69-5
• Molecular Formula: C₁₄H₁₈N₂O₃
• Molecular Weight: 262.309
• Mol file: 84408-69-5.mol

Synonyms:ethyl oxalate α-propylbenzylidenehydrazide

Chemical Property of ethyl oxalate α-propylbenzylidenehydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl oxalate α-propylbenzylidenehydrazide

There total 1 articles about ethyl oxalate α-propylbenzylidenehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propiophenone (495-40-9) + oxalic acid diethyl ester (95-92-1) → oxalic acid hydrazide (996-98-5) + oxalic acid α-propylbenzylidenehydrazid + ethyl oxalate α-propylbenzylidenehydrazide (84408-69-5)

Guidance literature:

With hydrazine hydrate; Yield given. Multistep reaction. Yields of byproduct given; 1) -15 deg C ethanol;

Reference yield:

meta-bromotoluene (591-17-3) + ethyl oxalate α-propylbenzylidenehydrazide (84408-69-5) → Hydroxy-di-m-tolyl-acetic acid [1-phenyl-but-(Z)-ylidene]-hydrazide (84408-72-0)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1) ether 2) reflux 1 h;

Reference yield:

1-bromo-butane (109-65-9) + ethyl oxalate α-propylbenzylidenehydrazide (84408-69-5) → 2-Butyl-2-hydroxy-hexanoic acid [1-phenyl-but-(E)-ylidene]-hydrazide (84408-82-2)

Guidance literature:

With magnesium; Yield given. Multistep reaction; 1) ether 2) reflux 1 h;

upstream raw materials:

propiophenone

oxalic acid diethyl ester

Downstream raw materials:

2-Butyl-2-hydroxy-hexanoic acid [1-phenyl-but-(E)-ylidene]-hydrazide

α-propylbenzylidenehydrazide of dimethylglycolic acid

2-Ethyl-2-hydroxy-butyric acid [1-phenyl-but-(E)-ylidene]-hydrazide

benzilic acid α-propylbenzylidenehydrazide

Refernces