phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

Base Information

Chemical Name:phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside
CAS No.:220587-65-5
Molecular Formula:C₄₇H₄₄N₂O₆Se
Molecular Weight:811.836
Hs Code.:

Synonyms:phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

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Chemical Property of phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

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Technology Process of phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

There total 3 articles about phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 728-15-4
(2,2-diphenylhydrazono)acetic acid

: 220587-64-4
phenyl 3,5,6-tri-O-benzyl-1-seleno-β-D-glucofuranoside

: 220587-65-5
phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 12h;
DOI:10.1021/jo981435w

Reference yield:

: 530-47-2,29666-92-0
N,N-diphenylhydrazine hydrochloride

: 220587-65-5
phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / H₂O / 2 h

2: 97 percent / DCC, DMAP / CH₂Cl₂ / 12 h

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; water;
DOI:10.1021/jo981435w

Reference yield:

: 220587-91-7
phenyl 2-O-acetyl-3,5,6-tri-O-benzyl-1-seleno-β-D-glucofuranoside

: 220587-65-5
phenyl 3,5,6-tri-O-benzyl-2-O-(diphenylhydrazono)-acetyl-1-seleno-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / K₂CO₃ / tetrahydrofuran; methanol / 0.25 h

2: 97 percent / DCC, DMAP / CH₂Cl₂ / 12 h

With dmap; potassium carbonate; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo981435w