(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

Base Information

Chemical Name:(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine
CAS No.:235094-10-7
Molecular Formula:C₁₉H₂₉NOSe
Molecular Weight:366.405
Hs Code.:

Synonyms:(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

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Chemical Property of (2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

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Technology Process of (2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

There total 2 articles about (2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 55179-51-6
(-)-aminomenthol

: 84782-51-4
α-phenylselenenyl propionaldehyde

: 235094-10-7
(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

: 235094-09-4
(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((R)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

Guidance literature:: In benzene; Ambient temperature;
DOI:10.1021/jo981693t

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 235094-10-7
(2S,4aS,7R,8aR)-4,4,7-Trimethyl-2-((S)-1-phenylselanyl-ethyl)-octahydro-benzo[e][1,3]oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / i-Pr₂NH / tetrahydrofuran / 1 h / Ambient temperature

2: 30 percent / benzene / Ambient temperature

With diisopropylamine; In tetrahydrofuran; benzene;
DOI:10.1021/jo981693t