Technology Process of C35H40O6Si
There total 3 articles about C35H40O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide;
In
tetrahydrofuran;
at 20 ℃;
for 25h;
Inert atmosphere;
DOI:10.1002/adsc.201100988
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 0 - 20 °C
1.2: 20 °C
2.1: water; acetic acid / 8 h / 20 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
4.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0 - 20 °C
5.1: copper(l) iodide / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere
With
1H-imidazole; copper(l) iodide; tetrabutylammomium bromide; water; acetic acid; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
5.1: Sonogashira coupling;
DOI:10.1002/adsc.201100988
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere
2: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0 - 20 °C
3: copper(l) iodide / tetrahydrofuran / 25 h / 20 °C / Inert atmosphere
With
1H-imidazole; copper(l) iodide; tetrabutylammomium bromide; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
3: Sonogashira coupling;
DOI:10.1002/adsc.201100988
