(10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Base Information

• Chemical Name: (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion
• CAS No.: 86814-84-8
• Molecular Formula: C₁₈H₂₁N₃O₈S₂
• Molecular Weight: 471.512

Synonyms:(10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Chemical Property of (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

There total 4 articles about (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

methanesulfonyl chloride (124-63-0) + (10R*,11R*)-10,11-Bis(hydroxymethyl)-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (86814-83-7) → (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (86814-84-8)

Guidance literature:

In pyridine; for 3h; 0 deg C to r.t.;

Reference yield:

trans 1,2-Dicarbethoxy-cyclohexa-3,5-dien (6268-45-7,32515-61-0,77803-86-2) → (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (86814-84-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 71 percent / LiAlH₄ / diethyl ether / Heating

2: 81 percent / acetone

3: 91 percent / pyridine / 3 h / 0 deg C to r.t.

With lithium aluminium tetrahydride; In pyridine; diethyl ether; acetone;

Reference yield:

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) → (10R*,11R*)-10,11-Bis<(methylsulfonyloxy)methyl>-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (86814-84-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / acetone

2: 91 percent / pyridine / 3 h / 0 deg C to r.t.

In pyridine; acetone;

upstream raw materials:

methanesulfonyl chloride

(10R*,11R*)-10,11-Bis(hydroxymethyl)-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

4-Phenyl-1,2,4-triazolidine-3,5-dione

trans-5,6-bis(hydroxymethyl)cyclohexa-1,3-diene

Downstream raw materials:

10,11-Dimethylen-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

6-Methyl-14-phenyl-4,6,8,12,14,16-hexaazapentacyclo<9.5.2.0^2,10.0^4,8.0^12,16>octadeca-2(10),17-dien-5,7,13,15-tetron

1,2,3,4-Tetrahydro-N-phenyl-2,3-phthalazindicarboximid

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