methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

Base Information

Chemical Name:methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide
CAS No.:79991-76-7
Molecular Formula:C₃₂H₃₆N₂O₁₀S
Molecular Weight:640.711
Hs Code.:

Synonyms:methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

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Chemical Property of methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

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Technology Process of methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

There total 5 articles about methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₃₁H₃₄N₂O₁₀S

: 74-88-4
methyl iodide

: 79991-76-7
methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

Guidance literature:: With potassium carbonate; In acetone; for 40h; Ambient temperature;
DOI:10.1021/jo00342a030

Reference yield:

: 4083-64-1
Tosyl isocyanate

: 79991-76-7
methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / Ambient temperature

2: 86 percent / K₂CO₃ / acetone / 40 h / Ambient temperature

With potassium carbonate; In acetone; acetonitrile;
DOI:10.1021/jo00342a030

Reference yield:

: 80010-07-7
methyl 3--3-deoxy-4-methyl-β-L-arabinopyranoside

: 79991-76-7
methyl 2-O-benzoyl-3-N-(benzyloxycarbonyl)-4-O-(N-methyltoluenesulfonylcarbamoyl)-β-garosaminide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 18 h / Ambient temperature

2: acetonitrile / Ambient temperature

3: 86 percent / K₂CO₃ / acetone / 40 h / Ambient temperature

With pyridine; potassium carbonate; In acetone; acetonitrile;
DOI:10.1021/jo00342a030