methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

Base Information

Chemical Name:methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside
CAS No.:85264-02-4
Molecular Formula:C₁₇H₂₆O₇S
Molecular Weight:374.455
Hs Code.:

Synonyms:methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

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Technology Process of methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

There total 4 articles about methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 124-63-0
methanesulfonyl chloride

: 85264-01-3
methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-α-D-galactopyranoside

: 85264-02-4
methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

Guidance literature:: With triethylamine; In dichloromethane; at -10 ℃; for 0.25h;
DOI:10.1007/BF00958405

Reference yield:

: 81076-77-9
1,6-anhydro-2-desoxy-2,4-di-C-methyl-3-O-benzyl-β-D-galactopyranose

: 85264-02-4
methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 17.2 percent / 3percent HCl / 3 h / Heating

2: 97 percent / Et₃N / CH₂Cl₂ / 0.25 h / -10 °C

With hydrogenchloride; triethylamine; In dichloromethane;
DOI:10.1007/BF00958405

Reference yield:

: 76706-48-4
1,6-anhydro-2-desoxy-2,4-di-C-methyl-β-D-galactopyranose

: 85264-02-4
methyl 2-desoxy-2,4-di-C-methyl-3-O-benzyl-6-O-mesyl-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: CH₃SOCH₂Na / dimethylsulfoxide / 1 h

2: 17.2 percent / 3percent HCl / 3 h / Heating

3: 97 percent / Et₃N / CH₂Cl₂ / 0.25 h / -10 °C

With hydrogenchloride; sodium methylsulfinylmethanide; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1007/BF00958405