N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

Base Information

Chemical Name:N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine
CAS No.:153815-19-1
Molecular Formula:C₃₉H₃₀FN₅O₇S
Molecular Weight:731.761
Hs Code.:

N<sup>6</sup>,N<sup>6</sup>-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

Synonyms:N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

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Technology Process of N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

There total 3 articles about N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 153815-18-0
C₃₉H₃₁N₅O₇S

: C₃₉H₃₁N₅O₈S

: 153815-19-1
N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

Guidance literature:: With xenon difluoride; In dichloromethane; at -60 ℃; for 6h; Yields of byproduct given;
DOI:10.1039/P19940000153

Reference yield:

: 2457-80-9
5'-Deoxy-5'-methylthioadenosine

: 153815-19-1
N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / 16 h / Ambient temperature

2: 75 percent / XeF₂ / CH₂Cl₂ / 6 h / -60 °C

With pyridine; xenon difluoride; In dichloromethane;
DOI:10.1039/P19940000153

Reference yield:

: 98-88-4
benzoyl chloride

: 153815-19-1
N⁶,N⁶-dibenzoyl-2',3'-O-dibenzoyl-5'-deoxy-5'-fluoromethylthioadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / 16 h / Ambient temperature

2: 75 percent / XeF₂ / CH₂Cl₂ / 6 h / -60 °C

With pyridine; xenon difluoride; In dichloromethane;
DOI:10.1039/P19940000153