2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone

Base Information

• Chemical Name: 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone
• CAS No.: 132028-98-9
• Molecular Formula: C₃₄H₃₀N₂O₄
• Molecular Weight: 530.623

Synonyms:2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone

Chemical Property of 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone

Chemical Property:

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Technology Process of 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone

There total 1 articles about 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-tert-Butylaniline (769-92-6) + 1,4,5,8-naphthalenetetracarboxylic dianhydride (81-30-1) → 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone (132028-98-9)

Guidance literature:

In N,N-dimethyl-formamide; for 12h; Reflux;

DOI:10.1021/acs.orglett.7b03861

Reference yield: 47.0%

2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone (132028-98-9) → 1,6-Bis-(4-tert-butyl-phenyl)-1H-indolo[5,4,3-def]isoquinoline-2,5,7-trione

Guidance literature:

With potassium hydroxide; In ethanol; at 90 - 100 ℃;

Reference yield: 11.0%

ethylenediamine (107-15-3,85404-18-8) + 2,7-bis(4-tert-butylphenyl)benzo[lmn][3,8]phananthroline-1,3,6,8-tetrone (132028-98-9) → 2-(4-tert-butylphenyl)benzo[lmn]imidazolo[1,2-j][3,8]phenanthroline-1,3,6-trione (887648-08-0) + N,N'-bis(4-tert-butylphenyl)-1,2,3,4-tetrahydronaphtho[2,3-b]pyrazine-5,6:9,10-bis(dicarboximide)

Guidance literature:

In N,N-dimethyl-formamide; Heating;

DOI:10.1002/chem.200500899

upstream raw materials:

4-tert-Butylaniline

1,4,5,8-naphthalenetetracarboxylic dianhydride

Downstream raw materials:

2-(4-tert-butylphenyl)benzo[lmn]imidazolo[1,2-j][3,8]phenanthroline-1,3,6-trione

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