D-TERT-LEUCINE HYDROCHLORIDE

Base Information

Chemical Name:D-TERT-LEUCINE HYDROCHLORIDE
CAS No.:112720-39-5
Molecular Formula:C₆H₁₃NO₂*ClH
Molecular Weight:167.636
Hs Code.:
Mol file:112720-39-5.mol

Synonyms:D-Valine,3-methyl-, hydrochloride (9CI);D-tert-Leucine hydrochloride;

Suppliers and Price of D-TERT-LEUCINE HYDROCHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(R)-2-Amino-3,3-dimethylbutanoicacidhydrochloride 95+%
5g
$ 564.00

American Custom Chemicals Corporation
D-TERT-LEUCINE HYDROCHLORIDE 95.00%
1G
$ 465.15

Total 38 raw suppliers

Chemical Property of D-TERT-LEUCINE HYDROCHLORIDE

Chemical Property:

Melting Point:>300°C
PSA：63.32000
LogP:1.94670
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

≥99% ^*data from raw suppliers

(R)-2-Amino-3,3-dimethylbutanoicacidhydrochloride 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-TERT-LEUCINE HYDROCHLORIDE

There total 11 articles about D-TERT-LEUCINE HYDROCHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: (R)-2-amino-3,3-dimethylbutanenitrile hydrochloride

: 112720-39-5
(R)-tert-leucine hydrochloride

Guidance literature:: With hydrogenchloride; at 100 ℃; for 40h;
DOI:10.1039/c8cc06658b

Reference yield:

: 1775-74-2
N-(2,2-dimethylpropylidene)benzylamine

: 112720-39-5
(R)-tert-leucine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: chiral salicylidene imine derivative / toluene / 15 h / -70 °C

1.2: Ac₂O / toluene

2.1: 99 percent / aq. H₂SO₄ / 20 h / 45 °C

3.1: aq. HCl / 12 h / 70 °C

4.1: H₂ / Pd/C / methanol

With hydrogenchloride; sulfuric acid; hydrogen; palladium on activated charcoal; chiral salicylidene imine derivative; In methanol; toluene; 1.1: Addition / 1.2: Formylation / 2.1: Hydrolysis / 3.1: Hydrolysis / 4.1: Hydrogenolysis;
DOI:10.1002/(SICI)1521-3773(20000403)39:7<1279::AID-ANIE1279>3.0.CO;2-U