(3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine

Base Information

• Chemical Name: (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine
• CAS No.: 1340483-84-2
• Molecular Formula: C₂₅H₃₅N₅
• Molecular Weight: 405.586

Synonyms:(3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine

Chemical Property of (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine

Chemical Property:

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Technology Process of (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine

There total 2 articles about (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + trimethylsilylazide (4648-54-8) + 3-diphenylpropyl amine (5586-73-2) + 1,1,3,3-tetramethylbutane isonitrile (14542-93-9) → (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine (1340483-84-2)

Guidance literature:

In methanol; at 80 ℃; for 1.5h; Inert atmosphere; Microwave irradiation; Sealed tube;

DOI:10.1016/j.bmc.2011.08.039

Reference yield: 86.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + trimethylsilylazide (4648-54-8) + 3-diphenylpropyl amine (5586-73-2) + 1,1,3,3-tetramethylbutane isonitrile (14542-93-9) → (3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine (1340483-84-2) + (3,3-diphenylpropyl)-bis-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine (1340483-78-4)

Guidance literature:

In methanol; at 80 ℃; for 1.5h; Inert atmosphere; Microwave irradiation; Sealed tube;

DOI:10.1016/j.bmc.2011.08.039

Reference yield: 65.0%

(3,3-diphenylpropyl)-[(1-(1,1,3,3-tetramethylbutyl)-1H-tetrazol-5-yl)methyl]amine (1340483-84-2) → (3,3-diphenylpropyl)-((1H-tetrazol-5-yl)methyl)amine hydrochloride (1340484-05-0)

Guidance literature:

With hydrogenchloride; In ethanol; for 8h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmc.2011.08.039

upstream raw materials:

formaldehyd

trimethylsilylazide

3-diphenylpropyl amine

1,1,3,3-tetramethylbutane isonitrile

Downstream raw materials:

(3,3-diphenylpropyl)-((1H-tetrazol-5-yl)methyl)amine hydrochloride

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