N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

Base Information

Chemical Name:N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride
CAS No.:1025952-00-4
Molecular Formula:C₁₄H₂₀ClNO₃S
Molecular Weight:317.837
Hs Code.:

Synonyms:N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

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Chemical Property of N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

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Technology Process of N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

There total 6 articles about N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 167867-25-6
(R)-2-<(tert-Butoxycarbonyl)amino>-1-phenylpropyl thioacetate

: 1025952-00-4
N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

Guidance literature:: With sulfuryl dichloride; acetic anhydride; In dichloromethane; at -20 - -5 ℃; for 1h;
DOI:10.1021/jo00121a038

Reference yield:

: 20312-36-1
L-3-phenyllactic acid

: 1025952-00-4
N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / SOCl₂ / 2 h / Ambient temperature

2: NH₃ / methanol

3: BH₃*THF / tetrahydrofuran / Heating

4: CH₂Cl₂ / 1 h / Ambient temperature

5: Ph₃P, DIAD / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) r.t., 1 h

6: Ac₂O, SO₂Cl₂ / CH₂Cl₂ / 1 h / -20 - -5 °C

With thionyl chloride; sulfuryl dichloride; borane-THF; di-isopropyl azodicarboxylate; ammonia; acetic anhydride; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00121a038

Reference yield:

: 69897-47-8
(S)-2-hydroxy-3-phenyl-propionamide

: 1025952-00-4
N-(tert-Butoxycarbonyl)-1(R)-benzylhypotauryl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: BH₃*THF / tetrahydrofuran / Heating

2: CH₂Cl₂ / 1 h / Ambient temperature

3: Ph₃P, DIAD / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) r.t., 1 h

4: Ac₂O, SO₂Cl₂ / CH₂Cl₂ / 1 h / -20 - -5 °C

With sulfuryl dichloride; borane-THF; di-isopropyl azodicarboxylate; acetic anhydride; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00121a038