N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

Base Information

Chemical Name:N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid
CAS No.:362057-65-6
Molecular Formula:C₂₄H₂₄NO₆P
Molecular Weight:453.431
Hs Code.:

Synonyms:N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

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Chemical Property of N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

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Technology Process of N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

There total 4 articles about N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 362057-76-9
ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

: 362057-65-6
N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

Guidance literature:: With sodium hydroxide; In ethanol;
DOI:10.1002/1099-0690(200107)2001:13<2559::AID-EJOC2559>3.0.CO;2-3

Reference yield:

: 17972-14-4
N-(3,4-dimethoxybenzylidene)methanamine

: 362057-65-6
N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / toluene / 1 h / Heating

2: 94 percent / triethylamine / toluene / 1 h / 0 °C

3: 95 percent / NaOH / ethanol

With sodium hydroxide; triethylamine; In ethanol; toluene;
DOI:10.1002/1099-0690(200107)2001:13<2559::AID-EJOC2559>3.0.CO;2-3

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 362057-65-6
N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / 4 Angstroem molecular sieves / toluene / 0 °C

2: 95 percent / toluene / 1 h / Heating

3: 94 percent / triethylamine / toluene / 1 h / 0 °C

4: 95 percent / NaOH / ethanol

With sodium hydroxide; 4 A molecular sieve; triethylamine; In ethanol; toluene;
DOI:10.1002/1099-0690(200107)2001:13<2559::AID-EJOC2559>3.0.CO;2-3