ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

Base Information

Chemical Name:ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate
CAS No.:362057-76-9
Molecular Formula:C₂₆H₂₈NO₆P
Molecular Weight:481.485
Hs Code.:

Synonyms:ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

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Chemical Property of ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

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Technology Process of ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

There total 2 articles about ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17972-14-4
N-(3,4-dimethoxybenzylidene)methanamine

: 362057-76-9
ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / toluene / 1 h / Heating

2: 94 percent / triethylamine / toluene / 1 h / 0 °C

With triethylamine; In toluene;
DOI:10.1002/1099-0690(200107)2001:13<2559::AID-EJOC2559>3.0.CO;2-3

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 362057-76-9
ethyl N-[(3,4-dimethoxyphenyl)(diphenylphosphinoyl)methyl]-N-methyloxalamate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 4 Angstroem molecular sieves / toluene / 0 °C

2: 95 percent / toluene / 1 h / Heating

3: 94 percent / triethylamine / toluene / 1 h / 0 °C

With 4 A molecular sieve; triethylamine; In toluene;
DOI:10.1002/1099-0690(200107)2001:13<2559::AID-EJOC2559>3.0.CO;2-3