4-(5-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOL-1-YL)ANILINE

Base Information

• Chemical Name: 4-(5-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOL-1-YL)ANILINE
• CAS No.: 1006348-64-6
• Molecular Formula: C₁₁H₁₀F₃N₃
• Molecular Weight: 241.216
• Hs Code.: 2921410090
• Mol file: 1006348-64-6.mol

Synonyms:4-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]aniline

Chemical Property of 4-(5-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOL-1-YL)ANILINE

Chemical Property:

• Boiling Point: 324.7±42.0 °C(Predicted)
• PKA: 3.02±0.10(Predicted)
• Density: 1.35±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

4-[5-Methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 4-(5-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOL-1-YL)ANILINE

There total 3 articles about 4-(5-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOL-1-YL)ANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.3%

5-methyl-1-(4-nitrophenyl)-3-(trifluoromethyl)pyrazole (374814-09-2) → 4-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]aniline (1006348-64-6)

Guidance literature:

With hydrogenchloride; at 20 ℃; for 4h;

Reference yield:

1,1,1-Trifluoro-2,4-pentanedione (367-57-7) → 4-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]aniline (1006348-64-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 70 °C

1.2: 2 h / 120 - 150 °C / Microwave irradiation

2.1: hydrogenchloride / 4 h / 20 °C

With hydrogenchloride; In ethanol;

Reference yield:

4-nitrophenylhydrazone (100-16-3) → 4-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]aniline (1006348-64-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 70 °C

1.2: 2 h / 120 - 150 °C / Microwave irradiation

2.1: hydrogenchloride / 4 h / 20 °C

With hydrogenchloride; In ethanol;

upstream raw materials:

5-methyl-1-(4-nitrophenyl)-3-(trifluoromethyl)pyrazole

4-nitrophenylhydrazone

1,1,1-Trifluoro-2,4-pentanedione

Downstream raw materials:

C₁₈H₁₃F₄N₃O

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